HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3,5-Dimethoxyphenyl)acetic acid → HCID 53239112, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3,5-Dimethoxyphenyl)acetic acid | HCID 138316 | — |
| Reactant | 2-amino-4-(4-chlorophenyl)phthalazin-1(2H)-one | HCID 67161367 | — |
| Product | HCID 53239112 | HCID 53239112 | — |
Reaction Steps
The product of Example 86A and 2-(3,5-dimethoxyphenyl)acetic acid were treated using a method similar to that described in Example 57 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.41-8.43 (m, 1H), 7.90-8.04 (m, 2H), 7.72-7.74 (m, 1H), 7.62-7.66 (m, 4H), 6.58 (d, J=2.3 Hz, 2H), 6.41 (t, J=2.3 Hz, 1H), 3.75 (s, 6H), 3.74 (s, 2H); MS (ESI−) M/Z 448 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-78a75cdc09964810bcab91d018159080 |
| Source note | uspto-grants-2014_01 |