Benzeneacetic acid, 4-bromo- → HCID 53238894, compound

Participants

Reaction Steps

The product of Example 86A and 2-(4-bromophenyl)acetic acid were treated using a method similar to that described in Example 57 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.40-8.44 (m, 1H), 7.93-8.04 (m, 2H), 7.72-7.75 (m, 1H), 7.60-7.67 (m, 4H), 7.54-7.57 (m, 2H), 7.34-7.36 (m, 2H), 3.69 (s, 2H); MS (ESI−) M/Z 466 (M−H)−.

Provenance & Evidence