p-Tolylacetic acid → HCID 53238889, compound

Participants

Reaction Steps

The product of Example 86A and 2-(4-methylphenyl)acetic acid were treated using a method similar to that described in Example 57 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.40-8.42 (m, 1H), 7.90-8.03 (m, 2H), 7.71-7.73 (m, 1H), 7.53-7.68 (m, 4H), 7.25-7.27 (m, 2H), 7.15-7.17 (m, 2H), 3.64 (s, 2H), 2.29 (s, 3H); MS (APCI+) M/Z 404 (M+H)+.

Provenance & Evidence