HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentylacetic acid → HCID 53238662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentylacetic acid | HCID 71606 | — |
| Reactant | 2-amino-4-(4-chlorophenyl)phthalazin-1(2H)-one | HCID 67161367 | — |
| Product | HCID 53238662 | HCID 53238662 | — |
Reaction Steps
The product of Example 86A and 2-cyclopentylacetic acid were treated using a method similar to that described in Example 57 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.40-8.43 (m, 1H), 7.88-8.04 (m, 2H), 7.73-7.75 (m, 1H), 7.59-7.69 (m, 4H), 2.33 (d, J=7.4 Hz, 2H), 2.16-2.28 (m, 1H), 1.75-1.87 (m, 2H), 1.59-1.69 (m, 2H), 1.49-1.58 (m, 2H), 1.19-1.31 (m, 2H); MS (ESI−) M/Z 380 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-758e8d163b054d84a6909f7ab908f4a1 |
| Source note | uspto-grants-2014_01 |