Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 469612Generated: October 30, 2026

4-Mesylphenylacetic acid → HCID 53238660, compound

https://huagongshe.com/reaction/469612

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Mesylphenylacetic acidHCID 572345—
Reactant2-amino-4-(4-chlorophenyl)phthalazin-1(2H)-oneHCID 67161367—
ProductHCID 53238660HCID 53238660—

Reaction Steps

The product of Example 86A and 2-[4-(methylsulfonyl)phenyl]acetic acid were treated using a method similar to that described in Example 57 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.40-8.43 (m, 1H), 7.95-8.02 (m, 2H), 7.90-7.94 (m, 2H), 7.72-7.75 (m, 1H), 7.65-7.68 (m, 2H), 7.61-7.66 (m, 4H), 3.86 (s, 2H), 3.20 (s, 3H); MS (ESI−) M/Z 466 (M−H)−.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08629143B2
Source datasetuspto-grants-2014_01
ORD IDord-27569f5b7254411a8475c837a0f87413
Source noteuspto-grants-2014_01