HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthaleneacetic Acid → HCID 67162542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthaleneacetic Acid | HCID 6862 | — |
| Reactant | 2-amino-4-(4-chlorophenyl)phthalazin-1(2H)-one | HCID 67161367 | — |
| Product | HCID 67162542 | HCID 67162542 | — |
Reaction Steps
The product from Example 86A and 2-(1-naphthyl)acetic acid were treated using a method similar to that described in Example 57 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.40-8.43 (m, 1H), 8.18 (d, J=8.2 Hz, 1H), 7.95-8.01 (m, 3H), 7.88 (d, J=8.1 Hz, 1H), 7.70-7.77 (m, 1H), 7.61-7.66 (m, 4H), 7.54-7.60 (m, 3H), 7.51 (dd, J=8.2, 7.1 Hz, 1H), 4.19 (s, 2H); MS (ESI−) M/Z 438 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-6ff75ead4ecb422fb54754b35ad9daca |
| Source note | uspto-grants-2014_01 |