HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,4,4-Trifluorobutanoic acid → HCID 67160313, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,4,4-Trifluorobutanoic acid | HCID 2777085 | — |
| Reactant | 2-amino-4-(4-chlorophenyl)phthalazin-1(2H)-one | HCID 67161367 | — |
| Product | HCID 67160313 | HCID 67160313 | — |
Reaction Steps
The product from Example 86A and 4,4,4-trifluorobutanoic acid were treated using a method similar to that described in Example 57 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.40-8.43 (m, 1H), 7.89-8.05 (m, 2H), 7.73-7.75 (m, 1H), 7.60-7.70 (m, 4H), 2.58-2.71 (m, 4H); MS (ESI−) M/Z 394 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-5425e3eddcfb4c0880e0077eb841d21a |
| Source note | uspto-grants-2014_01 |