(4-Chlorophenyl)acetic acid → HCID 53236387, compound

Participants

Reaction Steps

The product of Example 144A and 2-(4-chlorophenyl)acetic acid were treated using a method similar to that described in Example 17C to give the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.63 (s, 1H), 8.30 (d, J=8.3 Hz, 1H), 7.95-7.99 (m, 1H), 7.90-7.95 (m, 1H), 7.84-7.89 (m, 1H), 7.37-7.44 (m, 4H), 7.31-7.38 (m, 4H), 4.32-4.32 (bs, 2H), 3.70 (s, 2H); LC/MS (APCI) M/Z 438 (M+H)+.

Provenance & Evidence