3,5-Difluorophenylacetic acid → HCID 53236157, compound

Participants

Reaction Steps

The product of Example 144A and 2-(3,5-difluorophenyl)acetic acid were treated using a method similar to that described in Example 17C to give the title compound. 1H NMR (500 MHz, DMSO-d6) δ ppm 11.68 (s, 1H), 8.32 (dd, J=7.9, 1.4 Hz, 1H), 7.98 (d, J=7.9 Hz, 1H), 7.91-7.95 (m, 1H), 7.85-7.89 (m, 1H), 7.32-7.38 (m, 4H), 7.11-7.19 (m, 3H), 4.33 (s, 2H), 3.76 (s, 2H); LC/MS (APCI) M/Z 440 (M+H)+.

Provenance & Evidence