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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 469649Generated: October 30, 2026

3,5-Difluorophenylacetic acid → HCID 53236390, compound

https://huagongshe.com/reaction/469649

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,5-Difluorophenylacetic acidHCID 145424—
ReactantHCID 67161053HCID 67161053—
ProductHCID 53236390HCID 53236390—

Reaction Steps

The product of Example 159A and 2-(3,5-difluorophenyl)acetic acid were treated using a method similar to that described in Example 17C to give the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.67-11.81 (bs, 1H), 8.38-8.41 (m, 1H), 7.85-7.98 (m, 2H), 7.25-7.32 (m, 1H), 7.20-7.24 (m, 2H), 7.09-7.19 (m, 4H), 3.75 (s, 2H), 2.37 (s, 3H), 2.05 (s, 3H); MS (APCI+) M/Z 420 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08629143B2
Source datasetuspto-grants-2014_01
ORD IDord-339d53fea80646e7aaca7adcb1b58510
Source noteuspto-grants-2014_01