Hydrazine hydrate (1:1) → HCID 67160611, compound

HRID 469650Notes

Reaction equation

HRID 469650 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([CH:16]=[CH:17][C:18]=1[CH3:19])[C:5]([C:7]1[CH:15]=[CH:14][CH:13]=[CH:12][C:8]=1[C:9](O)=O)=O.[OH2:20].[NH2:21][NH2:22].C1(P(O[NH2:38])(C2C=CC=CC=2)=O)C=CC=CC=1>>[NH2:21][N:22]1[N:38]=[C:5]([C:4]2[CH:16]=[CH:17][C:18]([CH3:19])=[C:2]([CH3:1])[CH:3]=2)[C:7]2[C:8](=[CH:12][CH:13]=[CH:14][CH:15]=2)[C:9]1=[O:20]

Participants

4

Reactant 3

HCID 24654Hydrazine hydrate (1:1)HCID 3048682-(3,4-Dimethylbenzoyl)benzoic AcidHCID 10955453O-(Diphenylphosphinyl)hydroxylamine

Product 1

HCID 67160611HCID 67160611, compound

Procedure

2-(3,4-Dimethylbenzoyl)benzoic acid was treated with hydrazine hydrate using a method similar to that described in Example 11A, followed by treatment with O-(diphenylphosphoryl)hydroxylamine using a method similar to that described in Example 1B to give the title compound. MS (APCI+) M/Z 266 (M+H)+.

Sources & evidence

ORD record
ord-ae74ef2af4744b0187ec9a292a770762
Source dataset
uspto-grants-2014_01
Patent number
US08629143B2

Reaction notes

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