(4-Chlorophenyl)acetic acid → HCID 53236621, compound

Participants

Reaction Steps

The product of Example 163A and 2-(4-chlorophenyl)acetic acid were treated using a method similar to that described in Example 17C to give the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.69 (s, 1H), 8.38-8.40 (m, 1H), 7.88-8.02 (m, 2H), 7.74 (d, J=6.5 Hz, 1H), 7.38-7.44 (m, 4H), 7.33-7.36 (m, 1H), 7.27-7.33 (m, 2H), 3.70 (s, 2H), 2.32 (s, 3H), 2.31 (s, 3H); MS (APCI+) M/Z 418 (M+H)+.

Provenance & Evidence