3,5-Difluorophenylacetic acid → HCID 53236622, compound

Participants

Reaction Steps

The product of Example 168A and 2-(3,5-difluorophenyl)acetic acid were treated using a method similar to that described in Example 17C to give the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.70-11.81 (m, 1H), 8.40-8.42 (m, 1H), 7.89-8.03 (m, 2H), 7.75-7.78 (m, 1H), 7.51-7.53 (m, 2H), 7.43-7.46 (m, 2H), 7.07-7.22 (m, 3H), 3.77 (s, 2H), 2.94-3.07 (m, 1H), 1.27 (d, J=6.9 Hz, 6H); MS (APCI+) M/Z 434 (M+H)+.

Provenance & Evidence