HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 67161250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | O-(Diphenylphosphinyl)hydroxylamine | HCID 10955453 | — |
| Reactant | HCID 67160286 | HCID 67160286 | — |
| Reactant | HCID 178418365 | HCID 178418365 | — |
| Product | HCID 67161250 | HCID 67161250 | — |
Reaction Steps
The crude 2-tert-butyl-5-(trifluoromethyl)isoindoline-1,3-dione was treated with isopropylmagnesium bromide and hydrazine using a method similar to that described in Example 1A, followed by treatment with O-(diphenylphosphoryl)hydroxylamine using a method similar to that described in Example 1B to give the title compound. LC/MS (APCI) m/z 272 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-50cf0c1154274c1084aeaf8d5306bc1a |
| Source note | uspto-grants-2014_01 |