HRID47005

反应详情

EQUATION

反应方程式

HRID 47005 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 119 parts of 4'-chloro-2'-fluoroacetanilide in 475 parts of ethanol and 200 parts of 37% hydrochloric acid was refluxed for 17 hours and the solvent removed at a reduced pressure of 300 mm.Hg to yield the moist, solid hydrochloride salt of 4-chloro-2-fluoroaniline.

WORKUP

后处理

  1. temperaturewas refluxed for 17 hours
  2. customthe solvent removed at a reduced pressure of 300 mm.Hg