HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59784811, compound → HCID 59784760, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59784811 | HCID 59784811 | — |
| Reactant | HCID 178478477 | HCID 178478477 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 59784760 | HCID 59784760 | — |
Reaction Steps
A solution of salicylaldehyde derivative 1 (0.5 mmol) and diamine 2 (0.176 g, 0.5 mmol) in dimethylacetamide (4 mL) was stirred at 100° C. for 12 h. Solvent was evaporated and the residue was purified by preparative HPLC to give benzimidazole derivative 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629147B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-767a453eef514022b2180d55ee167413 |
| Source note | uspto-grants-2014_01 |