Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl 2-amino-3-nitrobenzoate | HCID 607264 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 59785142 | HCID 59785142 | — |
Reaction Steps
A suspension of 2-amino-3-nitro-benzoic acid methyl ester (785 mg, 4 mmol) and sodium hydroxide (194 mg, 4.4 mmol) in mixed solvent of EtOH (2 mL) and water (2 mL) was heated at 80° C. for 5 h. After it was cooled to the room temperature, the red colored precipitate was formed and dried at 40° C. under reduced pressure to afford the crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08629147B2 |
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| Source dataset | uspto-grants-2014_01 |
|---|
| ORD ID | ord-caf8c16fc8fa418cb254d2033f004cfe |
|---|
| Source note | uspto-grants-2014_01 |
|---|
