Ethanol → HCID 59785142, Verbindung

HRID 470345Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 470345
C[O:2][C:3](=[O:14])[C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([N+:10]([O-:12])=[O:11])[C:5]=1[NH2:13].[OH-].[Na+:16].CCO>O>[Na+:16].[NH2:13][C:5]1[C:6]([N+:10]([O-:12])=[O:11])=[CH:7][CH:8]=[CH:9][C:4]=1[C:3]([O-:14])=[O:2]

Komponenten

5

Edukt 3

HCID 702EthanolHCID 14798Sodium HydroxideHCID 607264Methyl 2-amino-3-nitrobenzoate

Produkt 1

HCID 59785142HCID 59785142, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Reaktionsbedingungen

Temperatur
80 °C

Versuchsvorschrift

A suspension of 2-amino-3-nitro-benzoic acid methyl ester (785 mg, 4 mmol) and sodium hydroxide (194 mg, 4.4 mmol) in mixed solvent of EtOH (2 mL) and water (2 mL) was heated at 80° C. for 5 h. After it was cooled to the room temperature, the red colored precipitate was formed and dried at 40° C. under reduced pressure to afford the crude product.

Aufarbeitung

  1. temperatureAfter it was cooled to the room temperature
  2. customthe red colored precipitate was formed
  3. customdried at 40° C. under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-caf8c16fc8fa418cb254d2033f004cfe
Quelldatensatz
uspto-grants-2014_01
Patentnummer
US08629147B2

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