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HRID47074

反应详情

EQUATION

反应方程式

HRID 47074 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)O
HCID176

Acetic Acid

C2H4O2

结构：O=C(C1CCCCO1)N1CCNCC1
HCID20385082

(Oxan-2-yl)(piperazin-1-yl)methanone

C10H18N2O2

结构：COc1cc2c(cc1OC)C(=CO)C(=O)N2
HCID178486553

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc2c(cc1OC)C(=CN1CCN(C(=O)C3CCCCO3)CC1)C(=O)N2
HCID53824958

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccccc1
溶剂HCID241

Benzene

C6H6

PROCEDURE

实验过程

5.00 g. of 5,6-dimethoxy-3-hydroxymethylene oxindole, 5,6 g. 1-(tetrahydropyran-2-carbonyl)piperazine and 2.1 g. acetic acid in 60 ml. benzene was reacted as described in Example 5 to give 6.18 g. of product, m.p. 208°-210° C.

WORKUP

后处理

  1. customto give 6.18 g