Allyl(4-methylphenyl) sulfide → HCID 14154894, compound

Participants

Reaction Steps

The title compound was prepared by a procedure similar to that described in Example 1 by reacting 2-(1H-imidazol-1-yl)-1-(3-methoxyphenyl)-N-methylethanimine N-oxide (1, R1 =3--OCH3) with allyl 4-methyphenyl sulfide (2: R2 =4--CH3). The resulting cis- and trans-diastereomeric mixture of compound 3 (R1 =3--OCH3, R2 =4--CH3, n=0) was flash-chromatographed on neutral silica gel using ethyl acetate as eluent.

Provenance & Evidence