HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-Chloroethane → 7,7-Dimethyl-2-phenethyl-5-(2-chloro-ethyl)-5H,7H-imidazo-[4,5-h]isoquinoline-4,6-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-Chloroethane | HCID 7849 | — |
| Reactant | HCID 70610353 | HCID 70610353 | — |
| Product | 7,7-Dimethyl-2-phenethyl-5-(2-chloro-ethyl)-5H,7H-imidazo-[4,5-h]isoquinoline-4,6-dione | HCID 70610648 | — |
Reaction Steps
Prepared analogous to Example 23 at room temperature from 4.3 gm of 7,7-dimethyl-2-phenethyl-5H,7H-imidazo[4,5-h]isoquinoline-4,6-dione and 2.2 gm of 2-bromo-1-chloro-ethane. The viscous oily crude product was directly further processed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04176184 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-022556f42d9a42c2ac9750cf99436ef9 |
| Source note | uspto-grants-1979_11 |