HCID 66693624, compound → HCID 86670267, compound

Participants

Reaction Steps

To a stirred solution of (5-methyl-7-p-tolylpyrazolo[1,5-a]pyrimidin-6-yl)methanol (300 mg, 1.18 mmol) in CH2Cl2 (24 mL) was added PCC (383 mg, 1.78 mmol). The reaction mixture was stirred at room temperature for 16 h. The solvent was evaporated and the residue was purified by silica gel chromatography to give the title compound (212 mg, 71.2%).

Provenance & Evidence