HRID47297

反应详情

EQUATION

反应方程式

HRID 47297 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
50 °C

PROCEDURE

实验过程

A mixture of 20 g 4-methoxybenzyl chloride, 26 g phthalimide potassium, and 100 ml dimethylformamide was stirred at 50° C. for 5 hr. After cooling, the reaction solution was poured into ice water and the resulting precipitates were collected by filtration. These were washed with water and dried to give 31 g of N-(4-methoxybenzyl)phthalimide.

WORKUP

后处理

  1. temperatureAfter cooling
  2. customthe resulting precipitates
  3. filtrationwere collected by filtration
  4. washThese were washed with water
  5. customdried