Lithium hydroxide, monohydrate → HCID 57572049, compound

HRID 473378Notes

Reaction equation

HRID 473378 reaction equation
[CH3:1][O:2][CH:3]([CH2:8][CH3:9])[C:4]([O:6]C)=[O:5].O.[OH-].[Li+:12]>CO.O>[CH3:1][O:2][CH:3]([CH2:8][CH3:9])[C:4]([O-:6])=[O:5].[Li+:12]

Participants

5

Reactant 2

HCID 168937Lithium hydroxide, monohydrateHCID 19792887Methyl 2-methoxybutanoate

Product 1

HCID 57572049HCID 57572049, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 962WaterSolvent

Procedure

In a 15-mL RBF was dissolved methyl 2-methoxybutanoate (0.027 g, 0.20 mmol) in methanol (0.75 mL). A solution of lithium hydroxide monohydrate (0.0086 g, 0.20 mmol) in water (0.75 mL) was added, and the mixture was stirred overnight. The mixture was concentrated to afford the title compound.

Workup

  1. concentrationThe mixture was concentrated

Sources & evidence

ORD record
ord-d10f5da4a5ec402682ade95236c7749e
Source dataset
uspto-grants-2014_01
Patent number
US08633315B2

Reaction notes

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