HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 58318606, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 58318609 | HCID 58318609 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 58318606 | HCID 58318606 | 115.3% |
Reaction Steps
2-(1-(3-Phenyl-1,5-naphthyridin-2-yl)ethyl)isoindoline-1,3-dione (120 mg, 0.32 mmol) was suspended in EtOH (2 mL) and treated with NH2NH2 (0.2 mL) at 70° C. for 30 min and worked up to give a colorless oil (92 mg, 96%). LC-MS (ESI) m/z 250 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633313B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-d22561f908a640829703ed8fd840ccc3 |
| Source note | uspto-grants-2014_01 |