HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → 2-Bromomethyl-3-methoxybenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 3-Methoxy-2-MethylBenzoic Acid | HCID 7021483 | — |
| Solvent | Chlorobenzene | HCID 7964 | — |
| Product | 2-Bromomethyl-3-methoxybenzoic acid | HCID 57058891 | — |
Reaction Steps
for the synthesis of the title compound, 6.64 g (0.040 mol) of 3-methoxy-2-methylbenzoic acid, 7.1 g (0.040 mol) of NBS and 0.25 g of AIBN in 150 ml of chlorobenzene are reacted by method H (variant 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633312B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-79c979a2b820446bb05861b3ac9a39bc |
| Source note | uspto-grants-2014_01 |