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HRID473463

反应详情

EQUATION

反应方程式

HRID 473463 的结构方程式

REACTANTS

反应物

3
结构：CC(C)(C#N)N=NC(C)(C)C#N
HCID6547

Azobisisobutyronitrile

C8H12N4

结构：O=C1CCC(=O)N1Br
HCID67184

1-Bromopyrrolidine-2,5-dione

C4H4BrNO2

结构：COc1cccc(C(=O)O)c1C
HCID7021483

3-methoxy-2-methylbenzoic acid

C9H10O3

PRODUCTS

生成物

1
结构：COc1cccc(C(=O)O)c1CBr
HCID57058891

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Clc1ccccc1
溶剂HCID7964

Chlorobenzene

C6H5Cl

PROCEDURE

实验过程

for the synthesis of the title compound, 6.64 g (0.040 mol) of 3-methoxy-2-methylbenzoic acid, 7.1 g (0.040 mol) of NBS and 0.25 g of AIBN in 150 ml of chlorobenzene are reacted by method H (variant 1).