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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 473467Generated: October 30, 2026

Hydrogen Bromide → HCID 67359866, compound

https://huagongshe.com/reaction/473467

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrogen BromideHCID 260—
ReactantHCID 67360944HCID 67360944—
SolventAcetic AcidHCID 176—
ProductHCID 67359866HCID 6735986695%

Reaction Steps

For the synthesis of the title compound, 1.0 (4.87 mmol) g of 8-chloro-1-methoxy-10,11-dihydrodibenzo[a,d]cyclohepten-5-one, 10 ml of HBr (48%, aqueous) and 10 ml of glacial acetic acid are employed in method L. Yield: 95%; m.p.: 185° C.; GC 15.2 min; C15H11ClO2 (Mr=258.71)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08633312B2
Source datasetuspto-grants-2014_01
ORD IDord-dd806ffd15d54fc5918262bc2c5aa02a
Source noteuspto-grants-2014_01