HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 67359866, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 67360944 | HCID 67360944 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 67359866 | HCID 67359866 | 95% |
Reaction Steps
For the synthesis of the title compound, 1.0 (4.87 mmol) g of 8-chloro-1-methoxy-10,11-dihydrodibenzo[a,d]cyclohepten-5-one, 10 ml of HBr (48%, aqueous) and 10 ml of glacial acetic acid are employed in method L. Yield: 95%; m.p.: 185° C.; GC 15.2 min; C15H11ClO2 (Mr=258.71)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633312B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-dd806ffd15d54fc5918262bc2c5aa02a |
| Source note | uspto-grants-2014_01 |