HRID473479

反应详情

EQUATION

反应方程式

HRID 473479 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

For the preparation of the title compound, 0.517 g (0.0020 mol) of 8-chloro-1-hydroxy-10,11-dihydrodibenzo[a,d]cyclohepten-5-one and 0.846 g (0.0030 mol) of Tf2O in 5 ml of pyridine are reacted by method R. C16H10ClF3O4S (Mr=390.77); GC 11.9 min