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HRID473480

反应详情

EQUATION

反应方程式

HRID 473480 的结构方程式

REACTANTS

反应物

3
结构：CO
HCID887

Methanol

CH4O

结构：O=S(=O)(O)O
HCID1118

Sulfuric acid

H2O4S

结构：Cc1cc([N+](=O)[O-])ccc1C(=O)O
HCID74790

4-Nitro-o-toluic acid

C8H7NO4

PRODUCTS

生成物

1
结构：COC(=O)c1ccc([N+](=O)[O-])cc1C
HCID15088700

Methyl 2-methyl-4-nitrobenzoate

C9H9NO4

PROCEDURE

实验过程

In accordance with general method S, 5.00 g (27.60 mmol) of 2-methyl-4-nitro-benzoic acid are dissolved in 20 ml of methanol, with heating, and 6 ml of concentrated sulfuric acid are added. The mixture is refluxed for 5 h. Yield: 4.90 g (90.9%); melting point: 73.6° C.

WORKUP

后处理

  1. temperaturewith heating
  2. temperatureThe mixture is refluxed for 5 h