HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 2-methyl-4-nitrobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 4-Nitro-o-toluic acid | HCID 74790 | — |
| Product | Methyl 2-methyl-4-nitrobenzoate | HCID 15088700 | — |
Reaction Steps
In accordance with general method S, 5.00 g (27.60 mmol) of 2-methyl-4-nitro-benzoic acid are dissolved in 20 ml of methanol, with heating, and 6 ml of concentrated sulfuric acid are added. The mixture is refluxed for 5 h. Yield: 4.90 g (90.9%); melting point: 73.6° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633312B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-83b26eea9aec47c9aac803c92db65d4b |
| Source note | uspto-grants-2014_01 |