HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67359760, compound → 3-Acetamido-8-nitro-6H-dibenzo[b,e]oxepin-11-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67359760 | HCID 67359760 | — |
| Solvent | Sulfolane | HCID 31347 | — |
| Product | 3-Acetamido-8-nitro-6H-dibenzo[b,e]oxepin-11-one | HCID 67360631 | — |
Reaction Steps
In accordance with general method W, 0.80 g (2.42 mmol) of (4) is partly dissolved in 10 ml of sulfolane at 100° C. 15 ml (30.0 g) of polyphosphoric acid are then added to the reaction mixture. Yield: 0.50 g (66.2%); melting point: 171.4° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633312B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-69d7417c44904d0f9810262a54dfbbb1 |
| Source note | uspto-grants-2014_01 |