HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous chloride dihydrate → 8-Amino-3-(2-methoxyphenylamino)-6H-dibenzo[b,e]oxepin-11-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous chloride dihydrate | HCID 61436 | — |
| Reactant | 3-(2-Methoxyphenylamino)-8-nitro-6H-dibenzo[b,e]oxepin-11-one | HCID 67362958 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 8-Amino-3-(2-methoxyphenylamino)-6H-dibenzo[b,e]oxepin-11-one | HCID 45280743 | — |
Reaction Steps
In accordance with general method Y, 0.10 g (0.44 mmol) of tin(II) chloride dihydrate is dissolved in 15 ml of ethanol, and 0.04 g (0.10 mmol) of (14) is added. Yield: 0.0046 g (13.3%); melting point: 68.4° C.; C21H18N2O3 (Mr=346.39); LC 18.55 min
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08633312B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-88f3c02542b0478aa4b53491bfa375c2 |
| Source note | uspto-grants-2014_01 |