HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178466839, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 3-Acetyl-4-methylthiobenzoic acid methyl ester | HCID 54514356 | — |
| Solvent | Methanol--water (1/1) | HCID 22242641 | — |
| Product | HCID 178466839 | HCID 178466839 | 79.8% |
Reaction Steps
3-acetyl4-methylthiobenzoic acid methyl ester (0.43 g) in water:methanol (1:3, 290 ml) containing sodium hydroxide (0.2 g) was stirred for 6 h. Methanol was removed at reduced pressure and the solution acidified with conc. hydrochloric acid to give 3-acetyl-4-methylthiobenzoic acid (0.32 g) after filtration. m/z (API+): 211 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06699879B1 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-1e9ebb6485c646609f456ce86dbd73b0 |
| Source note | uspto-grants-2004_03 |