Diisopropylethylamine → HCID 71529533, compound

Participants

Reaction Conditions

Reaction Steps

A tube was charged with 53 (63 mg, 0.27 mmol), 114 (44 mg, 0.27 mmol), DIPEA (2 mL) in IPA (5 mL), degassed, sealed and heated at 120° C. overnight. The solvent was evaporated in vacuo and the residue was purified by preparative HPLC to afford 56 mg (57%) of I-47 as white solid.

Provenance & Evidence