HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 475281Generated: October 29, 2026
Diisopropylethylamine → HCID 86694752, compound
https://huagongshe.com/reaction/475281
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 86694750 | HCID 86694750 | — |
| Reactant | HCID 178478345 | HCID 178478345 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 86694752 | HCID 86694752 | — |
Reaction Steps
A tube was charged with 264 (40 mg, 0.23 mmol), 53 (100 mg, 0.57 mmol), and DIPEA (0.3 ml) in IPA (3 mL), degassed, sealed and heated at 120° C. overnight. After removal of the solvent in vacuo, the crude was purified by preparative HPLC to afford 25 mg (29%) of I-95 as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08637537B2 |
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| Source dataset | uspto-grants-2014_01 |
|---|
| ORD ID | ord-746dd404613146aa9787b49b14918dde |
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| Source note | uspto-grants-2014_01 |
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