Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 475857Generated: October 31, 2026

HCID 58075657, compound → HCID 58075835, compound

https://huagongshe.com/reaction/475857

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58075657HCID 58075657—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 58075835HCID 5807583599.3%

Reaction Steps

To a solution of 2-chloro-4-(methylamino)-8-phenyl-7,8-dihydroquinazolin-8-ol (20 mg) in EtOAc (5 mL) was added 5% Pd/C (6 mg), and the resulting suspension was stirred under a hydrogen balloon for 1 h. The reaction mixture was filtered through a pad of Celite to give the title compound as a colorless oil (20 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08637525B2
Source datasetuspto-grants-2014_01
ORD IDord-7ab19487b56146cdb7433819e533e11b
Source noteuspto-grants-2014_01