Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Sulfite → Sodium 3-trifluoromethylbenzylsulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Sulfite | HCID 24437 | — |
| 반응물 | 3-(Trifluoromethyl)benzyl chloride | HCID 69716 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Sodium 3-trifluoromethylbenzylsulfonate | HCID 23700704 | 90.5% |
반응 단계
A mixture containing 50 g of 3-trifluoromethylbenzyl chloride and 32.4 g of sodium sulfite in 200 ml of water was refluxed for five hours and then concentrated by evaporation. The concentrate was then filtered to collect the precipitate (product). The precipitate was then washed with ethyl ether and then dried in a vacuum oven affording 61 g of sodium 3-trifluoromethylbenzylsulfonate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04885027 |
| 출처 데이터셋 | uspto-grants-1989_12 |
| ORD ID | ord-3035ba2ef0a1410d9769ed450dd25250 |
| 출처 메모 | uspto-grants-1989_12 |