Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Hexanol | HCID 8103 | — |
| Reactant | 87710-47-2 | HCID 353549 | — |
| Product | HCID 19838059 | HCID 19838059 | — |
Reaction Steps
A mixture of 2.5 g of 1,5-dihydro-5-hydroxy-2H-pyrrol-2-one in 75 cm3 of 1-hexanol and 1.3 g of Amberlite IR 120 H is heated to 85° C. for 2 hours. After allowing to cool to ambient temperature, the resin is filtered off and the solvent is evaporated under reduced pressure. The residue is distilled, and 3.4 g of the expected product is obtained. b.p. 120°-125° C. under 0.4 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04885307 |
|---|
| Source dataset | uspto-grants-1989_12 |
|---|
| ORD ID | ord-476efbf4b49e41cd86af0153b4677195 |
|---|
| Source note | uspto-grants-1989_12 |
|---|
