HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14771304, compound → 2-(Cyclohexyloxy)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14771304 | HCID 14771304 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(Cyclohexyloxy)aniline | HCID 14771305 | 90.7% |
Reaction Steps
Fifty ml of a methanol solution containing 3.7 g of 2-cyclohexyloxynitrobenzene and 0.2 g of 5% palladium on carbon was stirred at room temperature under a hydrogen atmosphere for catalytic reduction. The catalyst was removed by filtration, and the filtrate was evaporated off to give 2.9 g of 2-cyclohexyloxyaniline as pale brown crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04885367 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-84576895b9bb4a4fbcf6eb39bb9315ff |
| Source note | uspto-grants-1989_12 |