Calcium Chloride → HCID 67863945, compound

HRID 476747Notes

Reaction equation

HRID 476747 reaction equation
[CH:1]1([O:7][C:8]2[CH:13]=[C:12]([N+:14]([O-:16])=[O:15])[CH:11]=[CH:10][C:9]=2[NH:17][S:18]([CH3:21])(=[O:20])=[O:19])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[Na].[Cl-].[Ca+2:24].[Cl-]>C(O)C>[CH:1]1([O:7][C:8]2[CH:13]=[C:12]([N+:14]([O-:16])=[O:15])[CH:11]=[CH:10][C:9]=2[NH:17][S:18]([CH3:21])(=[O:20])=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1.[Ca:24]

Participants

4

Reactant 2

HCID 5284359Calcium ChlorideHCID 67863952HCID 67863952, compound

Product 1

HCID 67863945HCID 67863945, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

To 2 ml of an ethanol solution containing 0.2 g of sodium N-(2-cyclohexyloxy-4-nitrophenyl)methanesulfonamide obtained in Example 16 was added 0.6 ml of 1N calcium chloride at room temperature with stirring. The solvent was evaporated, and the resulting residue was recrystallized from water to give 0.17 g of calcium N-(2-cyclohexyloxy-4-nitrophenyl)methanesulfonamide.

Workup

  1. customThe solvent was evaporated
  2. customthe resulting residue was recrystallized from water

Sources & evidence

ORD record
ord-10ba82143d1b47eb8978903fadb8768d
Source dataset
uspto-grants-1989_12
Patent number
US04885367

Reaction notes

Loading…