Benzaldehyde → HCID 19838465, compound

HRID 476757Notes

Reaction equation

HRID 476757 reaction equation
Cl.[NH2:2][CH:3]1[CH2:15][C:14]2[C:6](=[CH:7][C:8]3[CH2:12][CH2:11][O:10][C:9]=3[CH:13]=2)[CH2:5][CH2:4]1.[CH:16](=O)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>C(O)C>[CH2:16]([N:2]=[C:3]1[CH2:15][C:14]2[C:6](=[CH:7][C:8]3[CH2:12][CH2:11][O:10][C:9]=3[CH:13]=2)[CH2:5][CH2:4]1)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

Participants

4

Reactant 2

HCID 240BenzaldehydeHCID 19838440HCID 19838440, compound

Product 1

HCID 19838465HCID 19838465, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

10 g of the compound of Example 2 are brought to reflux in 200 ml of ethanol in the presence of 2.8 g of benzaldehyde. A sample is removed, concentrated and recrystallized in ethanol.

Workup

  1. customA sample is removed
  2. concentrationconcentrated
  3. customrecrystallized in ethanol

Sources & evidence

ORD record
ord-97a89883145d4f20a5ee08fd0b789b69
Source dataset
uspto-grants-1989_12
Patent number
US04885373

Reaction notes

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