Sodium Carbonate → HCID 14234820, compound

HRID 476758Notes

Reaction equation

HRID 476758 reaction equation
Cl.[NH2:2][CH:3]1[CH2:15][C:14]2[C:6](=[CH:7][C:8]3[CH2:12][CH2:11][O:10][C:9]=3[CH:13]=2)[CH2:5][CH2:4]1.[CH2:16]([O:18][CH2:19][CH2:20]Br)[CH3:17].C(=O)([O-])[O-].[Na+].[Na+]>C(O)C>[CH2:16]([O:18][CH2:19][CH2:20][NH:2][CH:3]1[CH2:15][C:14]2[C:6](=[CH:7][C:8]3[CH2:12][CH2:11][O:10][C:9]=3[CH:13]=2)[CH2:5][CH2:4]1)[CH3:17]

Participants

5

Reactant 3

HCID 10340Sodium CarbonateHCID 611412-Bromoethyl ethyl etherHCID 19838440HCID 19838440, compound

Product 1

HCID 14234820HCID 14234820, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture containing 7.8 g of the compound of Example 2, 6.7 g of 2-bromoethyl ethyl ether and 6.2 g of sodium carbonate in ethanol is brought to reflux with stirring for 20 hours.

Workup

  1. temperatureto reflux

Sources & evidence

ORD record
ord-4bcdb6f992fb4207a2c78dc5b16c6de6
Source dataset
uspto-grants-1989_12
Patent number
US04885373

Reaction notes

Loading…