Hydrochloric Acid → HCID 19838480, compound

HRID 476760Notes

Reaction equation

HRID 476760 reaction equation
Cl.O.[O:3]1[C:7]2[CH:8]=[CH:9][C:10]([CH2:12][CH2:13][CH2:14][C:15](O)=O)=[CH:11][C:6]=2[CH2:5][CH2:4]1>[Zn].C1(C)C=CC=CC=1>[O:3]1[CH2:4][CH2:5][C:6]2[CH:11]=[C:10]3[C:9](=[CH:8][C:7]1=2)[CH2:15][CH2:14][CH2:13][CH2:12]3

Participants

6

Reactant 3

HCID 313Hydrochloric AcidHCID 962WaterHCID 10679778HCID 10679778, compound

Product 1

HCID 19838480HCID 19838480, compound

Reagents, catalysts & solvents 2

HCID 23994ZincCatalystHCID 1140TolueneSolvent

Procedure

An amalgam of zinc and mercuric chloride (72 g Zn and 7.1 g HgCL2) is added to a mixture containing 120 ml of concentrated hydrochloric acid, 57 ml of water, 30 g of the compound of Example 1 and 71 ml of toluene, with stirring.

Sources & evidence

ORD record
ord-16263ba1e6d04574b2d02f6525270c5a
Source dataset
uspto-grants-1989_12
Patent number
US04885373

Reaction notes

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