HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 14390154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl trifluoroacetate | HCID 9794 | — |
| Reactant | HCID 19838440 | HCID 19838440 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14390154 | HCID 14390154 | — |
Reaction Steps
A mixture containing 5 g of the compound of Example 2, 3.35 ml of triethylamine and 4 ml of ethyl trifluoroacetate in 7 ml of methanol is stirred for 4 hours at room temperature. The mixture is then evaporated to dryness and the dry residue obtained is recrystallized in isopropyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04885373 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-6a495e977a0244f9891818025b6f35bd |
| Source note | uspto-grants-1989_12 |