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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 476779Generated: October 25, 2026

13-Oxabicyclo[10.1.0]tridecane → Cyclododecanone

https://huagongshe.com/reaction/476779

Reaction equation

Participants

RoleNameHCIDCharge
Reactant13-Oxabicyclo[10.1.0]tridecaneHCID 9248—
ReactantLithium ChlorideHCID 433294—
ProductCyclododecanoneHCID 1324694%

Reaction Conditions

Temperature200 °C

Reaction Steps

25 g of epoxy-cyclododecane and 1 g of lithium chloride were dissolved in 20 g of N,N'-dimethyl ethylene urea and the solvent was stirred at 200° C. for 6 hours. The reaction mixture was analyzed to have a 94% yield of cyclododecanone.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04885397
Source datasetuspto-grants-1989_12
ORD IDord-7ae9b31cdbc147aa95cadb7d1820ee09
Source noteuspto-grants-1989_12