HRID476780

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID9248

13-Oxabicyclo[10.1.0]tridecane

C12H22O

HCID433294

Lithium chloride

ClLi

PRODUCTS

生成物

HCID13246

Cyclododecanone

C12H22O

收率 93.5%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID13387

N-Methyl-2-pyrrolidone

C5H9NO

CONDITIONS

反应条件

温度: 200 °C

PROCEDURE

实验过程

A solution containing 25 g of epoxy-cyclododecane, 1 g of lithium chloride, and 20 g of N-methyl-2-pyrrolidone was stirred at 200° C. for 6 hours. The reaction mixture contained 93.5% yield of cyclododecanone.