HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → Benzeneacetamide, 4-hydroxy-N-(phenylmethyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | Benzeneacetic acid, 4-hydroxy-, methyl ester | HCID 518900 | — |
| Product | Benzeneacetamide, 4-hydroxy-N-(phenylmethyl)- | HCID 8376026 | — |
Reaction Steps
A mixture of 80 g of 4-hydroxyphenylacetic acid methyl ester and 51.6 g of benzylamine is brought to 180° C. for 8 hours. The mixture is allowed to return to room temperature and the crystals are filtered off and washed with ethanol and then ethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04886799 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-467e9f33b6914da9b3e0388437aff99c |
| Source note | uspto-grants-1989_12 |