Benzoyl chloride → HCID 70378214, compound

HRID 476879Notes

Reaction equation

HRID 476879 reaction equation
[CH3:1][O:2][C:3]1[CH:11]=[C:10]2[C:6]([C:7]([CH2:12][CH2:13][N:14]3[CH2:19][CH2:18][NH:17][CH:16]([CH2:20][C:21]([O:23][CH2:24][CH3:25])=[O:22])[C:15]3=[O:26])=[CH:8][NH:9]2)=[CH:5][CH:4]=1.[C:27](Cl)(=[O:34])[C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1>C(N(CC)CC)C>[C:27]([N:17]1[CH2:18][CH2:19][N:14]([CH2:13][CH2:12][C:7]2[C:6]3[C:10](=[CH:11][C:3]([O:2][CH3:1])=[CH:4][CH:5]=3)[NH:9][CH:8]=2)[C:15](=[O:26])[CH:16]1[CH2:20][C:21]([O:23][CH2:24][CH3:25])=[O:22])(=[O:34])[C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1

Participants

4

Reactant 2

HCID 7412Benzoyl chlorideHCID 70378223HCID 70378223, compound

Product 1

HCID 70378214HCID 70378214, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Using the procedure of Step D of Example 1, 14 g of the product of Step C, 8.2 ml of triethylamine and 4.5 ml of benzoyl chloride were reacted to obtain 18 g of the expected product.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-9924b300665045aea5f08ea014b80383
Source dataset
uspto-grants-1989_12
Patent number
US04886802

Reaction notes

Loading…