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HRID477108

反应详情

EQUATION

反应方程式

HRID 477108 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)COc1ccc(CC(C)=O)cc1
HCID13851156

Methyl [4-(2-oxopropyl)phenoxy]acetate

C12H14O4

结构：Cc1nc(C(O)CN)cs1
HCID16768496

α-(Aminomethyl)-2-methyl-4-thiazolemethanol

C6H10N2OS

PRODUCTS

生成物

1
结构：COC(=O)COc1ccc(CC(C)NCC(O)c2csc(C)n2)cc1
HCID19974370

未命名化合物

PROCEDURE

实验过程

Prepared analogously to Example 13 by reaction of 2-hydroxy-2-(2-methyl-thiazol-4-yl)ethanamine with 1-(4-carbomethoxymethoxyphenyl)propan-2-one followed by purification of the base on a silica gel column using ethyl acetate/methanol=9:1 as eluant.

WORKUP

后处理

  1. customfollowed by purification of the base on a silica gel column